Hi Friends,
I am getting quite busy with my schedule, which is the reason I am not getting time to write my experiments. I will try to write them as soon as possible. Don’t worry I have them jotted down in my notes, but just not on the mahine. I will hopefully get them typed or probably write it on my own. Things are going good… Had my first chemical kick yesterday… The material frothed out of the condenser
. Anyways, wish me luck guys!! Bye!
JPV
Found a convinient methylation process. Going to try out that agaisnt the one with methly iodide… Here is the process…
Gallacetophenone 3,4-dimethyl ether
To a boiling mixture of gallacetophenone (16.8g, 1 mol), benzene (400 mL) and anhydrous K2CO3 (55g) was added methyl sulphate (26.5g, 2.05 mol) in one portion, and the whole refluxed for 6 h with occasional shaking. After the addition of water (750 mL) and shaking, the benzene layer was separated and shaken several times with NaOH solution, and the alkaline extracts solidified. The precipitated gallacetophenone 3,4-dimethyl ether after crystallisation from MeOH had mp 75-77°C (yield 10g) (for previous methods of preparation from gallacetophenone, see Perkin9, Perkin and Wilson10, David and von Kostanecki11).
I found this interesting. I think it should be easier
. The work up is much easier. No column atleast
What I am going to do from now on, is probably write down every thing I research. I will try to be as regular as I can be in the course of my writing. Let me begin with writing about the reaction that I carried out the other day. See you soon!
Hi, I need to confess, and regret that I have not been able to get all the content typed. Actually the images are taking a bit. I need to draw them so that you guys can use them. I am really sorry guys. I’ll try to make up for it in every way I can. Hope you guys keep reading this blog!
Hi, it’s been a while since I’ve been studying chemistry. chemistry has been my love, since the very beginning. Since the past few days in the run of life, I’ve never been able to actually concentrate and study chemistry. So this is my effort to keep myself updated in the field of chemistry. I will be writing every day. This is going to be my personal diary in the field of chemistry. and tried to keep as much records of what I have studied in this extra class. I have always been bad at attending classes. This is my effortto create an environment that I had missed for many days now. are really remember those days when I used to attendthe classes of chemistry in my college. I will surely be writing as much as I can, in keeping you poster on what I’m reading. I cope this blog helps you in the field at your studying currently. This is all I want to say right now! Hope to see you guys soon.
Hi,
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Thanks
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